2θ Cu-Kα Intensity [°] [a.u.] 10 0.621347744104262 10.1 0.656514914698354 10.2 0.635670469800879 10.3 0.658605884897837 10.4 0.649616725590202 10.5 0.657776469466044 10.6 0.634210156773814 10.7 0.663833225864943 10.8 0.661397320446215 10.9 0.658236339680986 11 0.654668548927808 11.1 0.659986021061896 11.2 0.674191524287993 11.3 0.67113363844026 11.4 0.677640618842069 11.5 0.680909239540998 11.6 0.672017934106057 11.7 0.674706836266802 11.8 0.696719422302972 11.9 0.686041180688947 12 0.698494291016475 12.1 0.709481639688814 12.2 0.701784280720601 12.3 0.719696972487883 12.4 0.73912246597268 12.5 0.708948967089237 12.6 0.723485123290813 12.7 0.725807439597696 12.8 0.719371557998062 12.9 0.710368027642634 13 0.719497439072339 13.1 0.742459642490096 13.2 0.736569922994846 13.3 0.753509084167691 13.4 0.7664171853185 13.5 0.761939522867037 13.6 0.746539435740411 13.7 0.795872361602691 13.8 0.780685615063425 13.9 0.755974862464448 14 0.776445613695458 14.1 0.765200990007654 14.2 0.792346343242741 14.3 0.774732249002299 14.4 0.804122487400143 14.5 0.790615530779074 14.6 0.816064888125456 14.7 0.828376677344652 14.8 0.809291487514555 14.9 0.827380449006789 15 0.815291288757948 15.1 0.809075571816373 15.2 0.84640102775107 15.3 0.830259410915761 15.4 0.832385605943361 15.5 0.858710108546784 15.6 0.820387652911201 15.7 0.852234038320312 15.8 0.847930472724486 15.9 0.848223846453245 16 0.87273002955699 16.1 0.868437461187431 16.2 0.878964834357209 16.3 0.875532418882177 16.4 0.880572268607173 16.5 0.876032634789225 16.6 0.895431521855864 16.7 0.878220214296249 16.8 0.89729184115938 16.9 0.902597652459535 17 0.899067263838968 17.1 0.873681020723723 17.2 0.936358530053037 17.3 0.904115186776739 17.4 0.906867245160645 17.5 0.895161651540613 17.6 0.923089900105613 17.7 0.939417183882075 17.8 0.921371238655459 17.9 0.904487810557627 18 0.923043263061238 18.1 0.934216962920791 18.2 0.938515854491231 18.3 0.927929172804933 18.4 0.946694273687788 18.5 0.950992207916184 18.6 0.93308918425332 18.7 0.94671243219608 18.8 0.942385945943453 18.9 0.936189560111015 19 0.92475655943509 19.1 0.919378183955586 19.2 0.947124716803396 19.3 0.946270061353105 19.4 0.945852583593909 19.5 0.934051929559273 19.6 0.955743259763944 19.7 0.963478099210033 19.8 0.965839146723369 19.9 0.948021523663719 20 0.958967518460646 20.1 0.959613179754332 20.2 0.968846415749984 20.3 0.971431136689306 20.4 0.958533406094673 20.5 0.988000979401222 20.6 0.958317622427194 20.7 0.985663798829795 20.8 0.976595151308065 20.9 0.979823860944239 21 0.986670371517267 21.1 0.993574181014411 21.2 0.991221434100652 21.3 0.969289508405381 21.4 0.970150048482102 21.5 0.949497086640807 21.6 0.974875108574849 21.7 0.964125792269638 21.8 0.961974658554438 21.9 0.979161229916884 22 0.947806863365744 22.1 0.948448173926907 22.2 0.959614040633811 22.3 1 22.4 0.97379282867434 22.5 0.994460305649459 22.6 0.988823267230395 22.7 0.997264198899638 22.8 0.989120435310291 22.9 0.988667889387719 23 0.96800749080266 23.1 0.981114152244965 23.2 0.945399653888661 23.3 0.948429451551651 23.4 0.944777772841195 23.5 0.944531663025449 23.6 0.932268497841684 23.7 0.96003974000086 23.8 0.938923332552353 23.9 0.930103112769475 24 0.930337435294675 24.1 0.930160346604284 24.2 0.900470945949593 24.3 0.895753142846908 24.4 0.913784673456903 24.5 0.894476629614179 24.6 0.884863823396609 24.7 0.890750950402952 24.8 0.868961963154943 24.9 0.859980456392798 25 0.867163363887619 25.1 0.873917264529429 25.2 0.834980018031998 25.3 0.837857867388488 25.4 0.831909124719151 25.5 0.841903746979937 25.6 0.79436429413786 25.7 0.773289294161852 25.8 0.792278155100463 25.9 0.769140783386355 26 0.763045740087409 26.1 0.771642672088196 26.2 0.746924635604423 26.3 0.747011123183782 26.4 0.75200313903343 26.5 0.725804104505721 26.6 0.713874404414514 26.7 0.678224706168121 26.8 0.683749445243734 26.9 0.688749028148599 27 0.656820938662507 27.1 0.639464221678813 27.2 0.649410480698591 27.3 0.635736134181252 27.4 0.637217999220322 27.5 0.625325270183699 27.6 0.619790496380254 27.7 0.595441076494948 27.8 0.592795824299326 27.9 0.580755663766031 28 0.574557792282695 28.1 0.548035126275766 28.2 0.550272803044536 28.3 0.551515182172407 28.4 0.541178310347231 28.5 0.531358758746404 28.6 0.51201534828973 28.7 0.509364068229824 28.8 0.517595265376234 28.9 0.50275336999418 29 0.488512433697106 29.1 0.479157079396175 29.2 0.469052598152936 29.3 0.48437192539962 29.4 0.474575176970847 29.5 0.461338642211441 29.6 0.447999635331267 29.7 0.435684947189148 29.8 0.448103341457106 29.9 0.43567048888291 30 0.437827476557576 30.1 0.422402404371881 30.2 0.42941740032506 30.3 0.409125354929096 30.4 0.415169793983213 30.5 0.416134816095881 30.6 0.386358914101178 30.7 0.415381092306785 30.8 0.408700879046741 30.9 0.419818020518157 31 0.382293998780962 31.1 0.390403028876901 31.2 0.38614308481812 31.3 0.379940645143388 31.4 0.367942295519844 31.5 0.361712018846519 31.6 0.373679412157774 31.7 0.371928910877434 31.8 0.355596395770967 31.9 0.356874563542016 32 0.35840671104576 32.1 0.350964832490421 32.2 0.35580476755885 32.3 0.354854290548861 32.4 0.347569665905928 32.5 0.350469736975528 32.6 0.354141797321074 32.7 0.334194764062925 32.8 0.332198357363267 32.9 0.35167290508305 33 0.327485389933699 33.1 0.333151678546958 33.2 0.325325790366793 33.3 0.335981077820588 33.4 0.328918158404194 33.5 0.33297344944675 33.6 0.318241414130007 33.7 0.319408243284482 33.8 0.311157090923212 33.9 0.328671466127878 34 0.335254399737196 34.1 0.315337849897627 34.2 0.309228753222555 34.3 0.31178911101838 34.4 0.296392700321148 34.5 0.308337565905415 34.6 0.323082528671644 34.7 0.321397702221644 34.8 0.31174259953355 34.9 0.314391775723815 35 0.29193277499653 35.1 0.296527172245646 35.2 0.286157425848874 35.3 0.288988925285655 35.4 0.311081141287981 35.5 0.319322651957624 35.6 0.305040358144583 35.7 0.308982008671612 35.8 0.309476395022284 35.9 0.304624082051116 36 0.311174322471499 36.1 0.304593634524493 36.2 0.308012884351088 36.3 0.303697477130905 36.4 0.310340060547225 36.5 0.316039512229096 36.6 0.285249114977873 36.7 0.291342028785562 36.8 0.305319559114166 36.9 0.286009510518837 37 0.283797134448521 37.1 0.291638169308805 37.2 0.284580257792829 37.3 0.296434132354182 37.4 0.289217059608568 37.5 0.290830482561542 37.6 0.297697478427601 37.7 0.308394729483961 37.8 0.293872380997592 37.9 0.289432411104926 38 0.289112480106516 38.1 0.277803430301603 38.2 0.296108307492018 38.3 0.303214906871827 38.4 0.294844255786957 38.5 0.290018710873493 38.6 0.305771071376488 38.7 0.28680517499258 38.8 0.282486847367874 38.9 0.293201257473813 39 0.287358525911639 39.1 0.277683458048043 39.2 0.284408281105303 39.3 0.288459707649272 39.4 0.291853781153537 39.5 0.285737250135189 39.6 0.279916903075185 39.7 0.282151248140622 39.8 0.266099098139695 39.9 0.272189911529688 40 0.259337331556952 40.1 0.282438326832765 40.2 0.282264424868281 40.3 0.27661510204859 40.4 0.274910713640291 40.5 0.275986605039248 40.6 0.268518988814306 40.7 0.261668122891137 40.8 0.263533703943325 40.9 0.267781035893317 41 0.264180409172214 41.1 0.252682558973191 41.2 0.262860729971979 41.3 0.261420960207619 41.4 0.263001240436949 41.5 0.271634702293614 41.6 0.264591940977157 41.7 0.247082027082787 41.8 0.274357806359877 41.9 0.256488532427801 42 0.275263936530218 42.1 0.260345501327818 42.2 0.271898217723213 42.3 0.264552872614625 42.4 0.258194583568216 42.5 0.257962142897003 42.6 0.260634755225968 42.7 0.254104383147174 42.8 0.249448383398845 42.9 0.252819971327317 43 0.251604934013068 43.1 0.250240695120372 43.2 0.252106321426566 43.3 0.252744712985159 43.4 0.258993928659158 43.5 0.244140219630137 43.6 0.250236187857688 43.7 0.252101815982415 43.8 0.253250414442926 43.9 0.254622283901412 44 0.229802469141467 44.1 0.255979614334082 44.2 0.239180028870873 44.3 0.231933561577385 44.4 0.238766557227295 44.5 0.23031161043393 44.6 0.253747192673999 44.7 0.225419709288295 44.8 0.230799166283077 44.9 0.218234979680619 45 0.23617862327786 45.1 0.225715725398223 45.2 0.23034706229115 45.3 0.225431466004792 45.4 0.21833014210012 45.5 0.214599674957372 45.6 0.217420769735458 45.7 0.21543653658864 45.8 0.21511606678197 45.9 0.226065244127669 46 0.20116679745433 46.1 0.211517285496495 46.2 0.225391983478135 46.3 0.217373920267703 46.4 0.210118974959708 46.5 0.212358318460144 46.6 0.198769431138279 46.7 0.201930905335864 46.8 0.210439660536372 46.9 0.20282598991021 47 0.202118030008967 47.1 0.197908025152847 47.2 0.198615850149632 47.3 0.194555845825414 47.4 0.196829616135869 47.5 0.186694644093402 47.6 0.20176233490466 47.7 0.18465617978685 47.8 0.197200181316441 47.9 0.194706336118577 48 0.181953696770456 48.1 0.174935087585499 48.2 0.188061502789588 48.3 0.181716420036638 48.4 0.183871235955692 48.5 0.170670678325704 48.6 0.192490499631907 48.7 0.177564701022073 48.8 0.179586735692751 48.9 0.164899671690801 49 0.182755878282753 49.1 0.168126696978503 49.2 0.171353722266206 49.3 0.182657743483176 49.4 0.172327108708578 49.5 0.155433730846874 49.6 0.175511469531633 49.7 0.167835248931938 49.8 0.163725530284752 49.9 0.154183597338927 50 0.155584182197251 50.1 0.169856347903332 50.2 0.153167538048216 50.3 0.14752517200385 50.4 0.152947109803264 50.5 0.157636037490349 50.6 0.142461751343961 50.7 0.145577611537894 50.8 0.140293890819827 50.9 0.151881060717187 51 0.140228573635109 51.1 0.14600831453061 51.2 0.133684576002417 51.3 0.144688648520888 51.4 0.149565491500523 51.5 0.135886794201792 51.6 0.14206780712605 51.7 0.1429933935816 51.8 0.137609606172654 51.9 0.145215186486809 52 0.137706240483596 52.1 0.132856795171822 52.2 0.137040338631272 52.3 0.130626356721206 52.4 0.134054482206258 52.5 0.139150731586961 52.6 0.116572310278552 52.7 0.132738158839622 52.8 0.126811136497234 52.9 0.129810246425927 53 0.125900210679043 53.1 0.127986080745386 53.2 0.126763701972489 53.3 0.116617679274507 53.4 0.119318437901024 53.5 0.120657976436785 53.6 0.0969406735163279 53.7 0.124557993751702 53.8 0.114287986385588 53.9 0.109797753589546 54 0.125185825176145 54.1 0.12201449985854 54.2 0.112656855703583 54.3 0.11599083207265 54.4 0.10729487895001 54.5 0.117629956625839 54.6 0.117526732104117 54.7 0.104745631104127 54.8 0.107293263399295 54.9 0.0981775908815413 55 0.107033736420799 55.1 0.125103386634016 55.2 0.102804733428065 55.3 0.11472893377615 55.4 0.107681747070013 55.5 0.112306892545159 55.6 0.0979199559715611 55.7 0.100174851187299 55.8 0.114108462362158 55.9 0.108501993849402 56 0.103492167323824 56.1 0.0930341508136834 56.2 0.104656649872127 56.3 0.0897773752277851 56.4 0.0967393137583616 56.5 0.105347788908851 56.6 0.0891917382926833 56.7 0.0817129125389309 56.8 0.0837219418423248 56.9 0.0816603652916987 57 0.0907782256462131 57.1 0.0880036494924702 57.2 0.090632668342437 57.3 0.0936701538327239 57.4 0.101942112238704 57.5 0.10439875467228 57.6 0.0762791318552207 57.7 0.0792338443095006 57.8 0.0788940011802883 57.9 0.0876875054471233 58 0.0942424242206334 58.1 0.091673348944535 58.2 0.079578145473493 58.3 0.0764049018859444 58.4 0.083595003409555 58.5 0.0775548539036602 58.6 0.0787538904093506 58.7 0.0880214650664078 58.8 0.0822406714447073 58.9 0.0764203243847041 59 0.0853571474581345 59.1 0.0767104424499011 59.2 0.0678737780405534 59.3 0.0766279119920457 59.4 0.0817570627333432 59.5 0.0848873724740503 59.6 0.0733251921186847 59.7 0.0639247301935101 59.8 0.0850041151780636 59.9 0.0743330251140057 60 0.0737556352342929 60.1 0.0704913478385694 60.2 0.0823644975464576 60.3 0.0689494531364541 60.4 0.0752252699939777 60.5 0.0748685874300106 60.6 0.0752685136353856 60.7 0.0661129093818543 60.8 0.0683019694796946 60.9 0.0661433328802313 61 0.0700970423173954 61.1 0.0660330916665275 61.2 0.0696655578071526 61.3 0.0543478576935343 61.4 0.0619184495550665 61.5 0.0697022309525112 61.6 0.0622365824474133 61.7 0.050575623896744 61.8 0.0717503706110765 61.9 0.0559913890530362 62 0.062486308689466 62.1 0.0685547433204478 62.2 0.0587237234378249 62.3 0.0613856085646196 62.4 0.0432265134646857 62.5 0.0681953769799072 62.6 0.0548672516458881 62.7 0.058058901852139 62.8 0.056835483824934 62.9 0.05597528962445 63 0.0508549871090087 63.1 0.058992988843597 63.2 0.0605477550927231 63.3 0.0616043893641788 63.4 0.0633398140148088 63.5 0.0526219196525633 63.6 0.0491952410148359 63.7 0.0555762233105616 63.8 0.0524487010116854 63.9 0.0572347359276566 64 0.0511024721855497 64.1 0.0528908913664004 64.2 0.0467031136939057 64.3 0.0508549871090087 64.4 0.0586290433512001 64.5 0.042208893286135 64.6 0.0540859097702469 64.7 0.0502645895381885 64.8 0.0486320967379797 64.9 0.0454082279108989 65 0.0560744030925532 65.1 0.0616690383671266 65.2 0.0492587047713559 65.3 0.0474986051821908 65.4 0.0455334444366029 65.5 0.0556423112242626 65.6 0.0586152438538667 65.7 0.0471343373833685 65.8 0.0561237662467692 65.9 0.0503283941618884 66 0.0532243303939167 66.1 0.0552136899733881 66.2 0.0530414160689036 66.3 0.0473460014055908 66.4 0.0510062402288977 66.5 0.0497143912324364 66.6 0.057216869465221 66.7 0.0375005067758912 66.8 0.0374418257660546 66.9 0.0544511708861277 67 0.0525345128225141 67.1 0.0531147723896545 67.2 0.0433178993839617 67.3 0.0374811143140445 67.4 0.0519215704223702 67.5 0.0393795992607465 67.6 0.0400852449048817 67.7 0.0421146417651711 67.8 0.0382942517493801 67.9 0.0295374983545752 68 0.0399892631572768 68.1 0.0491318283563484 68.2 0.0459940916216137 68.3 0.0513725932226649 68.4 0.0554442071800916 68.5 0.0437163537606398 68.6 0.0492520698957427 68.7 0.0359636998917579 68.8 0.040916784307988 68.9 0.0357193604374396 69 0.0413776139693769 69.1 0.0438704485650141 69.2 0.0423029931859109 69.3 0.0388897428700261 69.4 0.0456529592186423 69.5 0.0420575757389355 69.6 0.0266492603066828 69.7 0.0364235325554785 69.8 0.0348581277731321 69.9 0.0405703719493579 70 0.0475655610728314 70.1 0.0534522729320004 70.2 0.0397140509709996 70.3 0.0369819732616816 70.4 0.0464847687412833 70.5 0.0480233836877964 70.6 0.0447623034126683 70.7 0.0471619777023651 70.8 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