Pohl, Jean-MarieJean-MariePohlStöhr, FabianFabianStöhrKramer, TimTimKramerBecker, JonathanJonathanBeckerGöttlich, RichardRichardGöttlich2024-11-202024-11-202024https://jlupub.ub.uni-giessen.de/handle/jlupub/19867https://doi.org/10.22029/jlupub-19222A microwave-assisted synthesis of dialkyl and cyclic H-phosphonates via bis(2,2,2 trifluoroethyl) phosphonate (BTFEP) is described. This method enables the synthesis of various cyclic H-phosphonates and hetero-substituted dialkyl H-phosphonates by simple alcoholysis under non-inert and additive-free conditions. Short reaction times and the requirement for only stoichiometric amounts of alcohol render this method attractive for synthetic applications.enNamensnennung 4.0 Internationalddc:540